Case studies
Eastman chemical
Organization
Eastman Chemical Company
P.O. Box 7444
Longview, TX 75607
Equipment
Two isolation control valve systems in a high-pressure polyethylene plant
Objective
To improve valve reliability by the reduction of contamination and silting problems. Kidney loop filtration was added to the
system resevoirs. Halex Coils were used with the spin-on filters in the kidney loop systems.
Results
ISO cleanliness codes improved from 21/18 to 11/8 and from 18/11 to
12/8 in the two systems. Since the installation of the filtration system, no valves have stuck, but have responded as needed.
Scan of the lab results and correspondence with Eastman (1.10 MB
)
System 1
|
| Sample 0829 was taken upstream before the installation of Halex Coils. |
| Sample 0830 was taken downstream before the installation of Halex Coils. |
| Sample 0911 was taken upstream after the installation of Halex Coils. |
| Sample 0912 was taken downstream after the installation of Halex Coils. |
| Spectrographic analysis (ppm) |
Sample received |
Fe Iron |
Cr Chromium |
Mo Molybdenum |
Al Aluminum |
Cu Copper |
Pb Lead |
Sn Tin |
Ag Silver |
Ni Nickel |
Sb Antimony |
|
| 0829 |
1 |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
1 |
0 |
| 0830 |
1 |
0 |
1 |
0 |
0 |
1 |
0 |
0 |
1 |
0 |
| 0911 |
1 |
0 |
0 |
0 |
0 |
0 |
0 |
0 |
1 |
0 |
| 0912 |
1 |
0 |
0 |
0 |
1 |
0 |
0 |
0 |
0 |
0 |
|
| Spectrographic analysis (ppm) |
Sample received |
Ti Titanium |
Si Silicon |
Na Sodium |
K Potassium |
B Boron |
Mg Magnesium |
Ca Calcium |
Ba Barium |
P Phosphorus |
Zn Zinc |
|
| 0829 |
5 |
0 |
1 |
4 |
0 |
0 |
0 |
0 |
327 |
505 |
| 0830 |
0 |
0 |
2 |
4 |
0 |
0 |
0 |
0 |
305 |
482 |
| 0911 |
0 |
0 |
1 |
2 |
0 |
0 |
0 |
0 |
359 |
482 |
| 0912 |
0 |
2 |
0 |
1 |
0 |
0 |
0 |
0 |
385 |
482 |
|
| Physical properties |
Sample received |
% Fuel |
% Soot |
% Water |
Viscocity 40 °C |
Viscocity 100 °C |
TAN |
TBN |
|
| 0829 |
|
|
< 0.1 |
31.6 |
|
0.35 |
|
| 0830 |
|
|
< 0.1 |
31.0 |
|
0.38 |
|
| 0911 |
|
|
< 0.1 |
31.0 |
|
0.04 |
|
| 0912 |
|
|
< 0.1 |
31.0 |
|
0.08 |
|
|
| Physical properties |
Sample received |
Count ISO # |
PC/mL > 5 µm |
PC/mL > 10 µm |
PC/mL > 15 µm |
PC/mL > 20 µm |
PC/mL > 30 µm |
PC/mL > 40 µm |
|
| 0829 |
18/11 |
340 |
62 |
16 |
7 |
1 |
0 |
| 0830 |
15/12 |
214 |
60 |
23 |
12 |
3 |
1 |
| 0911 |
14/08 |
100 |
12 |
2 |
1 |
0 |
0 |
| 0912 |
12/08 |
33 |
10 |
3 |
1 |
1 |
0 |
|
| Physical properties |
Sample received |
IR Water |
IR Hydrocarbons |
IR Oxidation |
IR Nitration |
IR Glycol |
|
| 0829 |
1 |
717 |
1 |
0 |
1 |
| 0830 |
1 |
711 |
0 |
0 |
1 |
| 0911 |
0 |
733 |
1 |
0 |
1 |
| 0912 |
1 |
841 |
0 |
0 |
1 |
|
System 2
|
| Sample 0829 was taken upstream before the installation of Halex Coils. |
| Sample 0830 was taken downstream before the installation of Halex Coils. |
| Sample 0911 was taken upstream after the installation of Halex Coils. |
| Sample 0912 was taken downstream after the installation of Halex Coils. |
| Spectrographic analysis (ppm) |
Sample received |
Fe Iron |
Cr Chromium |
Mo Molybdenum |
Al Aluminum |
Cu Copper |
Pb Lead |
Sn Tin |
Ag Silver |
Ni Nickel |
Sb Antimony |
|
| 0829 |
0 |
0 |
1 |
0 |
1 |
0 |
1 |
0 |
2 |
0 |
| 0830 |
0 |
0 |
0 |
0 |
1 |
1 |
0 |
0 |
2 |
0 |
| 0911 |
0 |
0 |
0 |
0 |
1 |
0 |
0 |
0 |
1 |
0 |
| 0912 |
0 |
0 |
0 |
0 |
1 |
0 |
0 |
0 |
0 |
0 |
|
| Spectrographic analysis (ppm) |
Sample received |
Ti Titanium |
Si Silicon |
Na Sodium |
K Potassium |
B Boron |
Mg Magnesium |
Ca Calcium |
Ba Barium |
P Phosphorus |
Zn Zinc |
|
| 0829 |
0 |
0 |
1 |
4 |
0 |
0 |
0 |
0 |
314 |
544 |
| 0830 |
2 |
1 |
1 |
3 |
0 |
0 |
0 |
0 |
353 |
488 |
| 0911 |
0 |
2 |
0 |
2 |
0 |
0 |
53 |
0 |
371 |
475 |
| 0912 |
0 |
1 |
0 |
1 |
0 |
0 |
50 |
0 |
387 |
404 |
|
| Physical properties |
Sample received |
% Fuel |
% Soot |
% Water |
Viscocity 40 °C |
Viscocity 100 °C |
TAN |
TBN |
|
| 0829 |
|
|
< 0.1 |
31.4 |
|
0.33 |
|
| 0830 |
|
|
< 0.1 |
31.0 |
|
0.33 |
|
| 0911 |
|
|
< 0.1 |
32.0 |
|
0.17 |
|
| 0912 |
|
|
< 0.1 |
31.4 |
|
0.18 |
|
|
| Physical properties |
Sample received |
Count ISO # |
PC/mL > 5 µm |
PC/mL > 10 µm |
PC/mL > 15 µm |
PC/mL > 20 µm |
PC/mL > 30 µm |
PC/mL > 40 µm |
|
| 0829 |
20/10 |
15658 |
8713 |
1832 |
344 |
21 |
5 |
| 0830 |
16/14 |
387 |
174 |
112 |
81 |
4 |
1 |
| 0911 |
13/10 |
55 |
18 |
7 |
3 |
2 |
1 |
| 0912 |
11/08 |
15 |
6 |
2 |
1 |
0 |
0 |
|
| Physical properties |
Sample received |
IR Water |
IR Hydrocarbons |
IR Oxidation |
IR Nitration |
IR Glycol |
|
| 0829 |
1 |
685 |
2 |
1 |
1 |
| 0830 |
1 |
710 |
2 |
0 |
1 |
| 0911 |
1 |
780 |
4 |
2 |
1 |
| 0912 |
1 |
781 |
1 |
0 |
0 |
|